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Potassium methoxysalicylate

Potassium 4-methoxysalicylate

CAS: 152312-71-5

Molecular Formula: C8H7KO4

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Potassium methoxysalicylate - Names and Identifiers

Name Potassium 4-methoxysalicylate
Synonyms MSAK
4MSK
4-MSAK
4MS KTranexamic Acid
POTASSIUM METHOXYCINNAMATE
Potassium methoxysalicylate
Potassium 4-methoxysalicylate
POTASSIUM 4-METHOXYSALICYLATE
Potassium 2-hydroxy-4-methoxybenzoate
P-Methoxy salicylic acid potassium salt
Potassium methoxysalicylate Potassium 2-Hydroxy-4-methoxybenzoate
CAS 152312-71-5
InChI InChI=1/C8H8O4.K/c1-12-5-2-3-6(8(10)11)7(9)4-5;/h2-4,9H,1H3,(H,10,11);/q;+1/p-1

Potassium methoxysalicylate - Physico-chemical Properties

Molecular FormulaC8H7KO4
Molar Mass206.24
Melting Point>220°C (dec.)
Solubility DMSO (Slightly), Methanol (Slightly), Water (Slightly)
AppearanceAlmost white crystal or powder
ColorWhite to Off-White
Storage ConditionInert atmosphere,Room Temperature

Potassium methoxysalicylate - Reference Information

synthesis (1) will 2,4? Dihydroxybenzoic acid is slowly added into sodium hydroxide alkaline aqueous solution, and the temperature is controlled below 30 ℃, when 2,4? After all dihydroxybenzoic acid is added and dissolved, the temperature is lowered to 20 ℃, dimethyl sulfate is slowly added dropwise, the temperature is controlled below 40 ℃, after the dropwise is completed, the temperature is kept at 30~40 ℃ for 6 hours, after the reaction is over, the temperature is raised to 60 ℃, stirred for 30 minutes, the unreacted dimethyl sulfate is completely decomposed, then the temperature is lowered to normal temperature, the PH is adjusted to 1 with 10% hydrochloric acid, and a large amount of white solid substances are precipitated, centrifuge, rinse with deionized water, dry, get 4? Methoxysalicylic acid crude;
(2) 4? The crude methoxysalicylic acid is added to deionized water, heated to 80 ℃, stirred for 0.5 hours, filtered while hot, dried to obtain 4? Pure methoxysalicylic acid;
(3) in the deionized aqueous solution of potassium carbonate, raise the temperature to 50 ℃, slowly add 4? Methoxysalicylic acid, adjust PH = 7, stop adding 4? Methoxysalicylic acid, stirring for 30 minutes, starting to recover solvent, cooling crystallization, suction filtration, 4? Crude potassium methoxysalicylate;
(4) will 4? The crude potassium methoxysalicylate is dissolved in 50% ethanol solution, the activated carbon is decolorized for 40 minutes, suction filtration, cooling crystallization, vacuum drying, and 4? Pure methoxy potassium salicylate.
effect potassium 4-methoxysalicylate (potassium 4-methoxysalicylate) has a structure similar to salicylic acid. it is a new type of medicinal whitening ingredient, which is used in cosmetics and plays a whitening role. it is an effective ingredient of cosmetics. Potassium 4-methoxysalicylate can coordinate cutin metabolism, correct abnormal epidermal hyperplasia, promote the discharge of melanin, achieve skin smoothness and whitening; it can also block the source of melanin production and improve self-healing. It can be used in conjunction with various types of whitening products to improve the whitening effect and has good development prospects.
Last Update：2024-04-09 21:01:54
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View History
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